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Adlayer structures of pyridine base molecules over zeolite (010) surfaces: a semi-empirical study based on AFM observations

✍ Scribed by Komiyama, Masaharu; Shimaguchi, Takemi; Kobayashi, Mayumi; Wu, Hai-Ming; Okada, Takao


Book ID
101223151
Publisher
John Wiley and Sons
Year
1999
Tongue
English
Weight
117 KB
Volume
27
Category
Article
ISSN
0142-2421

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✦ Synopsis


The molecular array structures and molecular orientations within the adlayers of pyridine base molecules (pyridine and b-picoline) liquid-phase-adsorbed on (010) surfaces of natural zeolites (heulandite and stilbite) determined by in situ atomic force microscopy (AFM) were examined by semi-empirical molecular orbital calculations. All the adlayers studied possess (quasi-)hexagonal array structures, with di †erent two-dimensional lattice constants for di †erent adsorption systems. The AFM-observed array structures were close to the calculated energy minima with respect to their unit cell dimensions. The AFM-observed molecular orientation within the b-picoline adlayer was also energetically the most favourable among possible molecular orientations. Molecular tilt angles, which were not determined by AFM, were estimated by the semi-empirical calculations.