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Addition reactions of heterocyclic compounds. Part XXXIX. 2-Phenyl-ethynylpyridine and related pyridines with acetylenic esters

✍ Scribed by Acheson, R. M.; Bridson, J. N.


Book ID
120997545
Publisher
The Royal Society of Chemistry
Year
1969
Tongue
English
Weight
474 KB
Volume
8
Category
Article
ISSN
0022-4952

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## Experimental Section DMP (2.0 equiv) was added in one portion to a solution of 7 a (0.1 mmol) in benzene (4 mL) or BTF. [6] The solution was heated at reflux (or at 80 Β± 85 8C for the reactions in BTF) for about 30 min at which point TLC indicated complete consumption of starting material. Dilu