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Addition of HOXt (X = A or B) improves the efficiency of phenol-based coupling reagents during peptide synthesis

โœ Scribed by Ayman El-Faham


Book ID
105576514
Publisher
Springer Netherlands
Year
2000
Tongue
English
Weight
541 KB
Volume
7
Category
Article
ISSN
1573-3149

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An efficient scalable synthesis of 2-halothiazolium-type peptide coupling reagents has been developed. The key step is the formation of the 2-bromothiazole scaffold through cyclization of a-thiocyanato ketones with hydrogen bromide. Using this method, the new coupling reagent 2-bromo-N-methylthiazol