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Addition of Carbamoylsilanes to Electrophilically Substituted Alkenes. Preparation of β-Functionalized Tertiary Amides.

✍ Scribed by Robert F. Cunico; Adalie Rodriguez Motta

Publisher
John Wiley and Sons
Year
2005
Weight
46 KB
Volume
36
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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✍ Dr. Walter Brieden; Roswitha Ostwald; Prof. Dr. Paul Knochel 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 English ⚖ 407 KB 👁 1 views

To nBuLi (2.9 g. 46 mmol), constantly stirred at -8O"C, precooled pentane was added dropwise until a homogeneous solution was obtained (ca. 20 mL). After one week at -90 "C colorless blocks crystallized with a melting point of -34(2) 'C. rBuLi: tBuLi (2.2 g, 34 mmol) was treated as described for nBu