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Acetylation of unsymmetrical diols in the presence of Al2O3

✍ Scribed by Gary W. Breton; Melissa J. Kurtz; Sharyn L. Kurtz

Publisher
Elsevier Science
Year
1997
Tongue
French
Weight
240 KB
Volume
38
Category
Article
ISSN
0040-4039

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✦ Synopsis

The effect of the presence of chromatographic grade AI20 ~ on the acetylation of a series of unsymmetrical 1,5--diols was investigated. For diols containing both a primary and a secondary hydroxyl group, it was observed that higher yields of the more hindered secondary acelates were formed in the presence of A1203 than the corresponding reactions in solution.

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