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Acetals of lactams and acid amides. 46. Unusual reactions of α-cyano-β-dimethylaminocrotonamide with anthranilic acid derivatives

✍ Scribed by N. Z. Yalysheva; V. V. Chistyakov; V. G. Granik


Book ID
112356159
Publisher
Springer US
Year
1986
Tongue
English
Weight
335 KB
Volume
22
Category
Article
ISSN
0009-3122

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✍ L. V. Ershov; N. Z. Tugusheva; V. G. Granik 📂 Article 📅 1988 🏛 Springer US 🌐 English ⚖ 252 KB

N-Acetyl-2-(p-phenetidino)-3-cyano-5.~6~7,8-tetrahydroquinoline (lllg). A mixture of 1.92 g (0.01 mole) of (I) and 0.01 mole of N-acetyl-p-phenetidine was heated for 6 h at 190~ treated with hot water, and the solid filtered off and crystallized from ethanol to give 1.21 g (63%) of product, mp I15-I