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Acetals of lactams and acid amides. 42. Cyclization of dienamino esters, dienamino nitriles, and acylamidines to pyridine derivatives

โœ Scribed by N. I. Smetskaya; N. A. Mukhina; V. G. Granik


Book ID
111925135
Publisher
Springer US
Year
1984
Tongue
English
Weight
320 KB
Volume
20
Category
Article
ISSN
0009-3122

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Acetals of lactams and acid amides. 51.
โœ L. V. Ershov; N. Z. Tugusheva; V. G. Granik ๐Ÿ“‚ Article ๐Ÿ“… 1988 ๐Ÿ› Springer US ๐ŸŒ English โš– 252 KB

N-Acetyl-2-(p-phenetidino)-3-cyano-5.~6~7,8-tetrahydroquinoline (lllg). A mixture of 1.92 g (0.01 mole) of (I) and 0.01 mole of N-acetyl-p-phenetidine was heated for 6 h at 190~ treated with hot water, and the solid filtered off and crystallized from ethanol to give 1.21 g (63%) of product, mp I15-I