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Acetals of lactams and acid amides. 36. Some reactions of enamines of the isoquinoline series and synthesis of pyrimido[4,3-a]isoquinolines

โœ Scribed by V. G. Granik; V. F. Knyazeva; I. V. Persianova; N. P. Solov'eva; R. G. Glushkov

Book ID
112349153
Publisher
Springer US
Year
1982
Tongue
English
Weight
426 KB
Volume
18
Category
Article
ISSN
0009-3122

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6, 7, reacted similarly with hydroxylamine hydrochloride. The yields of oximes lllc and IVc in this case were 29% and 45%, respectively. 2-Phenyl-5-oxo-5,6~7~8-tetrahydroquinoline (V). This compound was obtained in 85% yield by the method in [3] from 3 g (0.0123 mole) of 2-[3-phenyl-3-oxopropyl]

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for 6 h at 600~ Directly before the experiment 50 ml of benzene was passed over at 550~ At the end of the addition of the starting compound, nitrogen was passed for another 30 rain, and the catalyzate was withdrawn and collected in a receiver with water cooling. 5-Vinylindole was isolated from the c