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Ab initio structure determination from severely overlapping powder diffraction data

โœ Scribed by Estermann, M. A. ;McCusker, L. B. ;Baerlocher, C.


Book ID
114500632
Publisher
International Union of Crystallography
Year
1992
Tongue
English
Weight
538 KB
Volume
25
Category
Article
ISSN
0021-8898

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Structure of ฮฑ-NaCaAlF6 determined ab in
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NaCaAIF6 is prepared by solid state reaction as poor quality crystals. The structure is determined ab initio from conventional X-ray powder data. The cell is monoclinic, space group P21/c, Z = 8, with a = 8.7423(3) A, b = 5.1927(2) A, c = 20.3514(9) A and 13 = 91.499(2) ยฐ. The final Rietveld refinem