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A Versatile Catalyst for the Sonogashira Coupling of Aryl Chlorides.

✍ Scribed by Axel Koellhofer; Thomas Pullmann; Herbert Plenio

Publisher
John Wiley and Sons
Year
2003
Weight
132 KB
Volume
34
Category
Article
ISSN
0931-7597

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Scheme 1. Synthesis of magnetic nanoparticle-supported (b-oxoiminato)(phosphanyl) palladium complex 4. a) NH 2 (CH 2 ) 3 Si(OEt) 3 , microwave heating; b) EtOTl, [Pd 2 (m-Cl) 2 Me 2 (PPh 3 ) 2 ], tetrahydrofuran, RT; c) tetraethyl orthosilicate; d) 2, toluene, 100 8C, 12 h.