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A two-step chemical and circular dichroic method for assigning the absolute configurations of sphingosines

✍ Scribed by Verena Dirsch; Justin Frederico; Ning Zhao; Guolin Cai; Yanqui Chen; Satyanarayana Vunnam; Joshua Odingo; Hyan Pu; Koji Nakanishi; Nina Berova; Dennis Liotta; Alicja Bielawska; Yusuf Hannun


Publisher
Elsevier Science
Year
1995
Tongue
French
Weight
271 KB
Volume
36
Category
Article
ISSN
0040-4039

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✍ Jinhai Gao; Hansjoerg Haas; Kate Yaping Wang; Zhuoliang Chen; Werner Breitenstei 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 377 KB

## Abstract We present here a new method using methoxyphenylacetic acid (MPA) as the chiral derivatizing agent (CDA) for the assignment of absolute configuration of cyclic secondary amines. The MPA amides were prepared using the purification‐free ‘mix and shake’ method. A detailed conformational an