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A Third-Generation Bicyclopropylidene: Straightforward Preparation of 15,15′-Bis(hexaspiro[2.0.2.0.0.0.2.0.2.0.1.0]pentadecylidene) and a C2v-Symmetric Branched [15]Triangulane

✍ Scribed by Malte von Seebach; Sergei I. Kozhushkov; Roland Boese; Jordi Benet-Buchholz; Dmitrii S. Yufit; Judith A. K. Howard; Armin de Meijere


Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
181 KB
Volume
39
Category
Article
ISSN
0044-8249

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By means of alternating current electrochemical synthesis crystals of [C 13 H 15 N 2 ] + 2 [CuCl 2.58 Br 1.42 ] ± (I) and [C 13 H 15 N 2 ] + [Cu 2 Cl 0.67 Br 2.33 ] ± (II) have been obtained and structurally characterized. Compound I crystallizes in the orthorhombic system, space group Fddd, a = 7.8

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