✦ LIBER ✦

A Thermodynamic Interpretation of Solubility of the Selected Higher Fatty Alcohols and Acids in Organic Solvents

✍ Scribed by Kowalska, T.

Publisher: John Wiley and Sons
Year: 1984
Weight: 354 KB
Volume: 86
Category: Article
ISSN: 0931-5985
DOI: 10.1002/lipi.19840860809

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✦ Synopsis

7.8. 8. 8.1. Losung Mar erscheint. Riickstande an den Kolbenwanden durch Umschwenken herunterspiilen. An-schlieBend nochmals 30 Min. lang nacherhitzen. Nach dem Abkuhlen des Aufschlusses auf Raumtemperatur die Losung vorsichtig mit 50 bis 80 ml Wasser versetzen und unter Nachspiilen mit Wasser in die Destillationsapparatur uberfiihren. Den Kiihlerauslauf der Destillationsapparatur in eine mit ca. 25 ml Borsaure-Losung und einigen Tropfen Indikator bescluckte Vorlage eintauchen. Nach Zugabe von ca. 70 ml Natronlauge die Wasserdampfdestillation beginnen. Vom Zeitpunkt des In&katorumschlages (von Rot nach Griin) nochmals 10 Min. lang destillieren.

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