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A synthesis of inside-inside bicyclics. A one step synthesis of [10] paracyclophanes.

✍ Scribed by Barry B. Snider; Nicholas J. Hrib

No coin nor oath required. For personal study only.

✦ Synopsis

We have recently described the aluminum chloride catalyzed 2+2 cycloaddition reaction of propiolate esters with mono-and l,%disubstituted alkenes.

Stirring methyl propiolate and 0.5 equiv. of aluminum chloride with a slight

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