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A structural study of peptides and proteins containing l-alanine residues by 13C NMR spectroscopy combined with ab initio chemical shift calculations

✍ Scribed by Naoki Asakawa; Hiromichi Kurosu; Isao Ando; Akira Shoji; Takuo Ozaki


Publisher
Elsevier Science
Year
1994
Tongue
English
Weight
829 KB
Volume
317
Category
Article
ISSN
0022-2860

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13C chemical shift tensors and secondary
✍ Naoki Asakawa; Masatoshi Takenoiri; Daisuke Sato; Minoru Sakurai; Yoshio Inoue πŸ“‚ Article πŸ“… 1999 πŸ› John Wiley and Sons 🌐 English βš– 180 KB πŸ‘ 2 views

Analyses of 13C chemical shielding tensors for powder samples of a-helix-rich poly-L-alanine (pALA) and the mechanically stretched b-sheet pALA Ðlms were performed by solid-state two-dimensional spin-echo (2DSE) NMR spectroscopy. From the iterative Ðtting of 2DSE spectra with spectrum simulations, i