## Abstract Preparation of a poly(styrene‐__co__‐divinylbenzene‐__co__‐methacrylic acid) monolithic stationary phase for the use in capillary electrochromatography (CEC) has been improved by optimizing the polymerization conditions. It is observed that the reaction time strongly affects column effi
✦ LIBER ✦
A strong inorganic acid-initiated methacrylate polymerization strategy for room temperature preparation of monolithic columns for capillary electrochromatography
✍ Scribed by Man-Man Wang; He-Fang Wang; Dong-Qing Jiang; Shan-Wei Wang; Xiu-Ping Yan
- Publisher
- John Wiley and Sons
- Year
- 2010
- Tongue
- English
- Weight
- 290 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0173-0835
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## Abstract A new vinyl aryl azide monomer, 4‐azidophenyl methacrylate (APM), has been synthesized and characterized by ^1^H NMR and FT‐IR spectroscopy. The thermal stability of APM has been investigated by temperature‐dependent FT‐IR spectroscopy and ^1^H NMR, and the monomer has been demonstrated