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A straightforward approach to unsaturated carboxylic acid derivatives starting from bis-silylated precursors

✍ Scribed by Annalisa De Girolamo; Vito Fiandanese; Giuseppe Marchese; Angela Punzi

Book ID
104208855
Publisher
Elsevier Science
Year
1998
Tongue
French
Weight
522 KB
Volume
54
Category
Article
ISSN
0040-4020

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✦ Synopsis

A new synthetic approach to substituted unsaturated carboxylic acid derivatives, such as amides, nitriles and esters, has been developed, starting from easily accessible bis-silylated precursors. The key step was based upon the reaction of a bis-silylated diene and a bis-silylated enyne with chlorosulphonyl isocyanate, which afforded mono-silylated amides, easily converted into substituted nitriles and esters.

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