A solid-state NMR study of the 2,15-dimethylhexadecane/urea inclusion compound
✍ Scribed by Thomas Handel; Falk Lissner; Thomas Schleid; Klaus Müller
- Publisher
- Elsevier Science
- Year
- 2007
- Tongue
- English
- Weight
- 699 KB
- Volume
- 837
- Category
- Article
- ISSN
- 0022-2860
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## Abstract For asymmetric guest molecules in urea, the end‐groups of two adjacent guest molecules may arrange in three different ways: head–head, head–tail and tail–tail. Solid‐state ^1^H and ^13^C NMR spectroscopy is used to study the structural properties of 1‐bromodecane in urea. It is found th
C NMR anisotropic chemical shielding spectra of the thiourea-ferrocene inclusion compound were measured between 125 and 294 K. The orientations and dynamic behaviour of ferrocene molecules trapped in the channels are discussed.