We demonstrate a dipolar-chemical shift correlation technique for sign-sensitive determination of the torsion angle in solid peptides and proteins under magic-angle spinning. The indirect dimension of the experiment is obtained by separate but synchronous evolution of the magnetization under the 15
✦ LIBER ✦
A Solid-State NMR 3D Heteronuclear Dipolar-Correlation Experiment. The Correlation of δ(13C), δ(15N), and DC-N
✍ Scribed by E.R.H. Vaneck; W.S. Veeman
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 224 KB
- Volume
- 109
- Category
- Article
- ISSN
- 1064-1858
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A variety of specialized probes are now available for the NMR characterization of small samples. The performance characteristics for 3 mm gradient micro inverse and 1.7 mm submicro inverse-detection gradient (SMIDG) NMR probes for the characterization of small samples using gradient inverse heteronu