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A Simplified and Convenient Laboratory-Scale Preparation of 14N or 15N High Molecular Weight Poly(dichlorophosphazene) Directly from PCl5.

✍ Scribed by Gabino A. Carriedo; Francisco J. Garcia Alonso; Paloma Gomez-Elipe; J. Ignacio Fidalgo; J. L. Garcia Alvarez; A. Presa-Soto

Publisher
John Wiley and Sons
Year
2003
Weight
87 KB
Volume
34
Category
Article
ISSN
0931-7597

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A Simplified and Convenient Laboratory-S
A Simplified and Convenient Laboratory-Scale Preparation of 14N or 15N High Molecular Weight Poly(dichlorophosphazene) Directly from PCl5
✍ Gabino A. Carriedo; Francisco. J. García Alonso; Paloma Gómez-Elipe; J. Ignacio 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 English ⚖ 84 KB

## Abstract A simple and convenient one‐pot synthesis of THF solutions of high molecular weight poly(dichlorophosphazene) [NPCl~2~]~__n__~, or the ^15^N isotopomer [^15^NPCl~2~]~__n__~, starting directly from PCl~5~ and NH~4~Cl or ^15^NH~4~Cl in a solution of 1,2,4‐trichlorobenzene in the presence