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A simple, rapid, isothermal gas chromatographic procedure for the analysis of monosaccharide mixtures

✍ Scribed by P.E. Reid; B. Donaldson; D.W. Secret; B. Bradford

Publisher
Elsevier Science
Year
1970
Tongue
English
Weight
909 KB
Volume
47
Category
Article
ISSN
1873-3778

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## Abstract A simple and rapid procedure for the preparation of [16,16‐^2^H~2~]‐and [16,16,17‐^2^H~3~]testosterone of high isotopic purity is described. [16,16‐^2^H~2~]DehydrOepiandrosterone is obtained by base‐catalysed exchange; reduction of the 17‐keto group using lithium aluminium hydride or li