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A simple radioisotopic assay for nucleoside kinases employing alumina for separation of nucleosides and nucleotides

✍ Scribed by Mahmoud H. el Kouni; Sungman Cha


Publisher
Elsevier Science
Year
1981
Tongue
English
Weight
388 KB
Volume
111
Category
Article
ISSN
0003-2697

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✦ Synopsis


A rapid, simple, and sensitive radiochemical assay for the measurement of purine or pyrimidine nucleoside kinases (EC 2.7. I .-) is described. The substrate (thymidine, deoxyuridine, deoxycytidine, deoxyguanosine, deoxyadenosine, uridine, cytidine, and adenosine) is separated from the product (the respective 5'-nucleotide) on neutral aluminacolumns which retain the nucleotides but not the nucleosides. The nucleotides are recovered by elution with 0.4 M sodium phosphate buffer, pH 7.6.