✦ LIBER ✦
A simple procedure for producing oxygen-labelled inorganic phosphate from isotopically labelled water that optimizes yield based on the isotope
✍ Scribed by William J. Ray Jr.
- Publisher
- John Wiley and Sons
- Year
- 1992
- Tongue
- French
- Weight
- 107 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0022-2135
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
Phosphorus pentachloride can be treated with stoichiometric amounts of oxygen‐labelled water to produce 80–90 percent yields of labelled inorganic phosphate when the reaction is conducted in dioxane. Any phosphorus‐chlorine bonds remaining at the end of the reaction are eliminated by reaction with diethylamine prior to adding water.