𝔖 Bobbio Scriptorium
✦   LIBER   ✦

A simple preparation of ethyl 2,5-dimethylfuran-3-carboxylate and 2,5-dimethylfuran-3,4-dicarboxylic acid from diethyl 2,3-diacetylsuccinate

✍ Scribed by Gang-Qiang Wang; Zhi Guan; Rong-Chang Tang; Zeljko Ostojic; T. Nicholas Jones; Ting-Ting Wu; Yan-Hong He

Publisher
Journal of Heterocyclic Chemistry
Year
2009
Tongue
English
Weight
88 KB
Volume
46
Category
Article
ISSN
0022-152X

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

magnified image

A simple preparation of ethyl 2,5‐dimethylfuran‐3‐carboxylate (3), 2,5‐dimethylfuran‐3,4‐dicarboxylic acid (4), and diethyl 2,5‐dimethylfuran‐3,4‐dicarboxylate (5) by treatment of diethyl 2,3‐diacetylsuccinate (2) with aqueous HCl is reported. The reaction is performed under organic solvent free conditions from a readily available cheap starting material. J. Heterocyclic Chem., (2009).

📜 SIMILAR VOLUMES

Synthesis of novel heterocycles from 2-a
Synthesis of novel heterocycles from 2-amino-3-cyanomethyl-sulfonyl-4,5-dimethylfuran
✍ Chad E. Stephens; J. Walter Sowell Sr. 📂 Article 📅 1997 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 303 KB 👁 1 views

## Abstract The synthesis and selected reactions of the versatile heterocycle 2‐amino‐3‐cyanomethylsulfonyl‐4,5‐dimethylfuran is reported. In particular, cyclization reaction of the aminofuran yielded a number of novel furo[3,2‐__b__]thiazine 1,1‐dioxides. Additionally, a novel tetracyclic system,

ChemInform Abstract: Optimized Synthesis
ChemInform Abstract: Optimized Synthesis and Simple Purification of 2,5-Diamino-thiophene-3,4-dicarboxylic Acid Diethyl Ester.
✍ Marie Bourgeaux; Sophie Vomscheid; W. G. Skene 📂 Article 📅 2008 🏛 John Wiley and Sons ⚖ 20 KB 👁 1 views

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable v