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A simple oxidative procedure for the removal of ruthenium residues from metathesis reaction products

✍ Scribed by David W. Knight; Ian R. Morgan; Anthony J. Proctor

Publisher
Elsevier Science
Year
2010
Tongue
French
Weight
209 KB
Volume
51
Category
Article
ISSN
0040-4039

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Alternative and mild procedures for the
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✍ Philippe Renaud; Emmanuel LacΓ΄te; Laura Quaranta πŸ“‚ Article πŸ“… 1998 πŸ› Elsevier Science 🌐 French βš– 191 KB

Simple treatment of tributyltin halide-containing reaction mixtures with Me3AI or aq. IM NaOH leads after filtration through silica gel to complete removal of tin residues. The Me3AI method is particularly convenient for polar products and the NaOH method for non-polar products.