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A simple method for the synthesis of 5-isoxazolyl-4-thioxo-1,3,5-benzoxadiazocines

✍ Scribed by E. Rajanarendar; E. Kalyan Rao; A. Siva Rami Reddy

Publisher
Journal of Heterocyclic Chemistry
Year
2009
Tongue
English
Weight
80 KB
Volume
46
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

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Synthesis of novel isoxazolyl 1,3,5‐benzoxadiazocines 5 has been accomplished by condensation of 3‐amino‐5‐methylisoxazole 1 with salicylaldehydes, followed by reduction, treatment with arylisothiocyanates, and subsequent ring closure in the presence of formaldehyde. The methodology used in this synthesis is the first approach of its kind. J. Heterocyclic Chem., 46, 134 (2009).

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