A simple method for the preparation and selective functionalization of 4,5-diaminopyrazoles
โ Scribed by Benjamin E Blass; Anil Srivastava; Keith R Coburn; Amy L Faulkner; William L Seibel
- Publisher
- Elsevier Science
- Year
- 2003
- Tongue
- French
- Weight
- 155 KB
- Volume
- 44
- Category
- Article
- ISSN
- 0040-4039
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โฆ Synopsis
A simple procedure for the synthesis and further functionalization of 4,5-diaminopyrazoles using mild conditions is reported herein. The desired products were obtained in good yield, and the structures have been confirmed by X-ray crystallography.
๐ SIMILAR VOLUMES
The structure of product (8) follows from its cleavage by acid to cyclohexanone (2,4-dinitrophenylhydrazone, m.p. 162 "C) and 4-phenylsemicarbazide (benzylidene derivative, m. p. and mixed n1.p. 180ยฐC).
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