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A simple method for NMR probe tuning and some consequences of improper probe tuning

✍ Scribed by P Daugaard; H.J Jakobsen; A.R Garber; P.D Ellis


Publisher
Elsevier Science
Year
1981
Weight
470 KB
Volume
44
Category
Article
ISSN
0022-2364

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## Abstract A simple method is reported for temperature calibration of a magic angle spinning probe for solid‐state NMR spectroscopy. The method is an extension of that developed by van Geet for temperature calibration of liquid‐state NMR probes, and consists of measuring the frequency difference (