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A simple method for determining non-ortho substituted PCBs in Kanechlors, Aroclors and environmental samples

✍ Scribed by Narayanan Kannan; Shinsuke Tanabe; Tadaaki Wakimoto; Ryo Tatsukawa


Book ID
119022146
Publisher
Elsevier Science
Year
1987
Tongue
English
Weight
147 KB
Volume
16
Category
Article
ISSN
0045-6535

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A simple and rapid hydride generationβ€”at
✍ R.G. Smith; J.C. Van Loon; J.R. Knechtel; J.L. Fraser; A.E. Pitts; A.E. Hodges πŸ“‚ Article πŸ“… 1977 πŸ› Elsevier Science 🌐 English βš– 581 KB

An inexpensive 50-ml disposable (hypodermic) syringe is used as the arsine generation vessel. The arsine is passed into a lo-cm long. lo-mm i.d. electrically heated silica tube atomizer with nitrogen carrier gas. Jkcess of hydrogen is burned off in a hydrogen diffusion flame at the ends of the tube.