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A simple and convenient preparation of succinic semialdehyde

✍ Scribed by Enzo Santaniello; Ada Manzocchi


Publisher
Elsevier Science
Year
1980
Tongue
English
Weight
254 KB
Volume
108
Category
Article
ISSN
0003-2697

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✦ Synopsis


Succinic semialdehyde (SSA) is prepared from 4-pentenoic acid by ozonolysis and reductive decomposition of the formed ozonide (40-W% yields). Aqueous solutions of SSA are obtained by water extraction from ethyl acetate solution of the mixture of reaction. Quantitative estimation of SSA was performed enzymatically by means of SSA dehydrogenase.


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Preparation of deuteriated succinic acid
✍ Masashi Tashiro; Hirohisa Tsuzuki; Shin-Ichiro Isobe; Hideyuki Goto; Shoji Ogasa πŸ“‚ Article πŸ“… 1991 πŸ› John Wiley and Sons 🌐 French βš– 361 KB

## Abstract Succinic [2,3‐^2^H~2~]‐ and [2,2,3,3‐^2^H~4~]‐acids were prepared from maleic anhydride and dimethyl fumarate, and acetylene dicarboxylic acid and its dimethyl ester by treatment with CuAl and Ni‐Al alloys in 10% NaOD‐D~2~O in 95% to 100% isotopic purity. The succinic ^2^H~4~ acid havin