A simple and convenient preparation of succinic semialdehyde
β Scribed by Enzo Santaniello; Ada Manzocchi
- Publisher
- Elsevier Science
- Year
- 1980
- Tongue
- English
- Weight
- 254 KB
- Volume
- 108
- Category
- Article
- ISSN
- 0003-2697
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β¦ Synopsis
Succinic semialdehyde (SSA) is prepared from 4-pentenoic acid by ozonolysis and reductive decomposition of the formed ozonide (40-W% yields). Aqueous solutions of SSA are obtained by water extraction from ethyl acetate solution of the mixture of reaction. Quantitative estimation of SSA was performed enzymatically by means of SSA dehydrogenase.
π SIMILAR VOLUMES
## Abstract Succinic [2,3β^2^H~2~]β and [2,2,3,3β^2^H~4~]βacids were prepared from maleic anhydride and dimethyl fumarate, and acetylene dicarboxylic acid and its dimethyl ester by treatment with CuAl and NiβAl alloys in 10% NaODβD~2~O in 95% to 100% isotopic purity. The succinic ^2^H~4~ acid havin