✦ LIBER ✦

A selective pulse sequence for the determination of long-range C,H spin coupling constants

✍ Scribed by M. Findeisen; S. Berger

Publisher: John Wiley and Sons
Year: 2003
Tongue: English
Weight: 140 KB
Volume: 41
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1184

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✦ Synopsis

Abstract

A new pulse sequence for determining scalar long range C,H spin couplings in small organic molecules is proposed. It is based on the combination of a selective J‐resolved spectrum with a selective HMBC and displays the long‐range spin couplings of one chosen carbon atom in the indirect dimension. Advantages and disadvantages are discussed on example spectra of ethanol, strychnine and sucrose. Copyright © 2003 John Wiley & Sons, Ltd.

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