A novel 90 degrees composite pulse sequence which allows one to record 1D and 2D NMR spectra without disturbing the water magnetization is described. A home-written program was used to optimize the pulse angles for which the pulse sequence response fitted best the desired excitation profile, produci
✦ LIBER ✦
A pulse sequence which provides rapid, routine 1H13C shift-correlated spectra
✍ Scribed by William F Reynolds; Donald W Hughes; Marion Perpick-Dumont; Raul G Enriquez
- Publisher
- Elsevier Science
- Year
- 1985
- Weight
- 470 KB
- Volume
- 64
- Category
- Article
- ISSN
- 0022-2364
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## Abstract The application of a Hahn spin–echo extended X–^1^H shift‐correlated (X = ^13^C, ^29^Si, ^119^Sn, ^207^Pb) two‐dimensional NMR technique to carbon–, silicon–, tin– and lead–nitrogen compounds is described. This allows complete suppression of the central line (representing the isotopomer