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A Practical Method for the Disposal of Organotin Residues from Reaction Mixtures

✍ Scribed by Salomon, Claudio J.; Danelon, Gerardo O.; Mascaretti, Oreste A.


Book ID
127024938
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
36 KB
Volume
65
Category
Article
ISSN
0022-3263

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Simple treatment of tributyltin halide-containing reaction mixtures with Me3AI or aq. IM NaOH leads after filtration through silica gel to complete removal of tin residues. The Me3AI method is particularly convenient for polar products and the NaOH method for non-polar products.