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A Practical and Highly Efficient Synthesis of Lennoxamine (VIIa) and Related Isoindolobenzazepines.

โœ Scribed by Poolsak Sahakitpichan; Somsak Ruchirawat

Publisher
John Wiley and Sons
Year
2004
Weight
105 KB
Volume
35
Category
Article
ISSN
0931-7597

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A new approach to isoindolobenzazepines
A new approach to isoindolobenzazepines via a ring-expansion of isoindoloisoquinoline: Synthesis of lennoxamine and chilenine
โœ Yuji Koseki; Shuichi Kusano; Harumi Sakata; Tatsuo Nagasaka ๐Ÿ“‚ Article ๐Ÿ“… 1999 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 217 KB

A convenient short-step synthesis of lennoxamine 1 and chilenine 2 is described. The key steps are the preparation of an acyliminium ion precursor and a novel expansion of the six-membered ring to a seven-membered ring.