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A Practical and Efficient Synthesis of the C-16—C-28 Spiroketal Fragment (CD) of the Spongistatins.

✍ Scribed by Matthew J. Gaunt; David F. Hook; Huw R. Tanner; Steven V. Ley

Publisher
John Wiley and Sons
Year
2004
Weight
62 KB
Volume
35
Category
Article
ISSN
0931-7597

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Short Diastereoselective Synthesis of the C1–C13 (AB Spiroacetal) and C17–C28 Fragments (CD Spiroacetal) of Spongistatin 1 and 2 through Double Chain-Elongation Reactions
✍ Dr. Christopher L. Flowers; Prof. Dr. Pierre Vogel 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 370 KB

## Abstract A unique and practical synthetic sequence for rapid access to polyketides and to further the spiroacetals derived from them, which utilizes a bidirectional Hosomi–Sakurai allylation approach around key allylsilanes in the synthesis of the AB and CD ring systems of spongistatin 1 and 2,