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A novel synthesis of precursors to 3-thienylmalonic acid

โœ Scribed by Peter W. Raynolds

Book ID
112127579
Publisher
Journal of Heterocyclic Chemistry
Year
1984
Tongue
English
Weight
119 KB
Volume
21
Category
Article
ISSN
0022-152X

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Synthesis of 3-aminoaspartic acid deriva
Synthesis of 3-aminoaspartic acid derivatives from glycine precursors
โœ Yu Chen; Andrei K. Yudin ๐Ÿ“‚ Article ๐Ÿ“… 2003 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 133 KB

3-Aminoaspartic acid derivatives 3 have been synthesized via stereoselective alkylation of a-acetyloxyglycine Schiff base 2 with the enolate of glycine anion equivalent 1 as a carbon nucleophile in the presence of Pd(OAc) 2 and BINAP at room temperature. High chemical yields and moderate stereoselec