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A Novel Synthesis of Isothiocyanates from Amines Using Triphenylphosphine/Carbon Tetrachloride

✍ Scribed by Furukawa, Isao; Abe, Noboru; Hashimoto, Shizunobu


Book ID
121263233
Publisher
Informa UK (Taylor & Francis)
Year
1987
Weight
61 KB
Volume
30
Category
Article
ISSN
0308-664X

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πŸ“œ SIMILAR VOLUMES


A new efficient synthesis of isothiocyan
✍ Henrik Munch; Jon S. Hansen; Michael Pittelkow; JΓΈrn B. Christensen; Ulrik Boas πŸ“‚ Article πŸ“… 2008 πŸ› Elsevier Science 🌐 French βš– 115 KB

Alkyl and aryl amines are converted smoothly to the corresponding isothiocyanates via the dithiocarbamates in good to excellent yields using di-tert-butyl dicarbonate (Boc 2 O) and 1-3 mol % of DMAP or DABCO as catalyst. As most of the byproducts are volatile, the work-up involves simple evaporation

ChemInform Abstract: A New Efficient Syn
✍ Henrik Munch; Jon S. Hansen; Michael Pittelkow; Joern B. Christensen; Ulrik Boas πŸ“‚ Article πŸ“… 2008 πŸ› John Wiley and Sons βš– 30 KB πŸ‘ 2 views

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a β€œFull Text” option. The original article is trackable v