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A novel ring contraction: 3β-methyl-A-nor-5β-cholestan-5-ol-6-one from 3β-tosyloxy-5α-cholestane-5,6β-diol through an ene reaction of an unsaturated acyloin

✍ Scribed by D.S. Brown; R.W.G. Foster; B.A. Marples; K.G. Mason


Publisher
Elsevier Science
Year
1980
Tongue
French
Weight
123 KB
Volume
21
Category
Article
ISSN
0040-4039

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✦ Synopsis


Sa-cholestane-5,6B_dlol with B&K/B&H, * This doublet is clearly resolved in the 3COMHz spectrum but only the up-field branch is resolved in the 9OMHs spectrum.