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A Novel Reductive Cyclization of Arylidenecyanoacetate Induced by the TiCl4/Sm System.

✍ Scribed by Daqing Shi; Hong Zhao; Xiangshan Wang; Changsheng Yao; Longhu Zhou

Publisher
John Wiley and Sons
Year
2003
Weight
80 KB
Volume
34
Category
Article
ISSN
0931-7597

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Simultaneous reduction of the nitro grou
Simultaneous reduction of the nitro group and the azide group in o-nitrophenylazide induced by the TiCl4/Sm system: a novel synthesis of 2,3-dihydro-1H-1,5-benzodiazepines
✍ Weihui Zhong; Yongmin Zhang; Xiaoyuan Chen πŸ“‚ Article πŸ“… 2001 πŸ› Elsevier Science 🌐 French βš– 76 KB

o-Nitrophenylazide was treated with the low-valent titanium reagent derived from the TiCl 4 /Sm system to produce the intermediate 2 in situ, which was a 'living' double-anion and reacted readily with ketones containing active methyl or methylene groups to afford 2,3-dihydro-1H-1,5-benzodiazepines i

ChemInform Abstract: Simultaneous Reduct
ChemInform Abstract: Simultaneous Reduction of the Nitro Group and the Azide Group in o-Nitrophenylazide Induced by the TiCl4/Sm System: A Novel Synthesis of 2,3-Dihydro-1H-1,5-benzodiazepines.
✍ Weihui Zhong; Yongmin Zhang; Xiaoyuan Chen πŸ“‚ Article πŸ“… 2001 πŸ› John Wiley and Sons βš– 33 KB πŸ‘ 2 views

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