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A novel aldehyde synthesis based on a “nucleophilic carbene” of the s-triazole series, and a new method for the degradation ofα-hydroxyacids.

✍ Scribed by Gábor Doleschall

Publisher
Elsevier Science
Year
1975
Tongue
French
Weight
196 KB
Volume
16
Category
Article
ISSN
0040-4039

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A new method for the synthesis of α-thio
A new method for the synthesis of α-thio aldehydes and alcohols from aldehydes with one-carbon elongation
✍ Tsuyoshi Satoh; Ko-ichi Kubota 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 148 KB

A two-step and high-yield method for the synthesis of α-thio aldehydes from aldehydes with one-carbon elongation is realized by using chloromethyl phenyl sulfoxide as a one-carbon homologating agent. The α-thio aldehydes are easily converted to desulfurized alcohols with Bu 3 SnH and AIBN in refluxi