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A Non-Catalyst Method for the Synthesis of Bis-4-aryl-3,4-dihydropyrimidones (thiones) under Solvent-Free Conditions

โœ Scribed by Mukhopadhyay, Chhanda; Datta, Arup


Book ID
125485198
Publisher
Japan Institute of Heterocyclic Chemistry
Year
2010
Tongue
English
Weight
1014 KB
Volume
81
Category
Article
ISSN
0385-5414

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Zirconium(IV) 4-sulphophenylethyliminobi
โœ Xin-Bin Yang; Xiang-Kai Fu; Yu Huang; Ren-Quan Zeng ๐Ÿ“‚ Article ๐Ÿ“… 2011 ๐Ÿ› Versita ๐ŸŒ English โš– 194 KB

## Abstract Zirconium(IV) 4-sulphophenylethyliminobismethylphosphonate (ZSBEDP) was prepared and characterised by elemental analysis, IR, TG-DSC, and XRD. ZSBEDP was found to be an efficient catalyst for the Biginelli reaction of aromatic aldehyde, ethyl acetoacetate, and urea or thiourea under sol