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A new synthetic route to 3,5-diphenyl-4-pyridones

✍ Scribed by Ibrahim El-Sayed El-Kholy; Morcos Michael Mishrikey; Ragheb Fuad Atmeh


Book ID
112123008
Publisher
Journal of Heterocyclic Chemistry
Year
1973
Tongue
English
Weight
142 KB
Volume
10
Category
Article
ISSN
0022-152X

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✍ Anthonyβ€…J. Bellamy; Simonβ€…J. Ward; Peter Golding πŸ“‚ Article πŸ“… 2002 πŸ› John Wiley and Sons 🌐 English βš– 378 KB πŸ‘ 2 views

A new, three-stage synthesis of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) has been developed which avoids the use of halogenated precursors or reagents. The starting material, 1,3,5trihydroxy-benzene, is converted via the sequence nitrationalkylation-amination to TATB in an overall yield of 87%. T