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A New Preparation of the Disaccharide β‐ D ‐ManNAc p ‐(1 → 4)‐ D ‐Glc from Lactose Through a Highly Stereoselective β‐ D ‐Gal p to β‐ D ‐ManNAc p Transformation

✍ Scribed by Attolino, Emanuele; Catelani, Giorgio; D'Andrea, Felicia; Nicolardi, Maria

Book ID
126863490
Publisher
Taylor and Francis Group
Year
2004
Tongue
English
Weight
188 KB
Volume
23
Category
Article
ISSN
0732-8303

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Synthesis of Protected Hexp-(1 → 4)-β-D-
Synthesis of Protected Hexp-(1 → 4)-β-D-GlcpNAc-(1 → 2)-α-D-Manp-(1 → O)(CH2)7CH3 sequences (hex = β-D-Glc, 4-deoxy-4-fluoro-β-D-Gal, or 4-deoxy-β-D-Gal) Using a Glc–GlcNPhth Donor, Eventually Fluorinated or Deoxygenated at the Oligosaccharide Level
✍ van Dorst, Johannes A. L. M. ;Voskamp, Anton F. ;Kamerling, Johannis P. ;Vliegen 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 866 KB

## Abstract Three trisaccharide derivatives of the type β‐D‐Hex__p__‐(1 → 4)‐β‐D‐Glc__p__NAc(1 → 2)‐α‐D‐Man__p__‐(1 → O)(CH~2~)~7~CH~3~ have been synthesized, with Hex being either glucose (15), 4‐deoxy‐4‐fluorogalactose (20), or 4‐deoxygalactose (27). These trisaccharides have been designed for th

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✍ J. A. L. M. VAN DORST; A. F. VOSKAMP; J. P. KAMERLING; J. F. G. VLIEGENTHART 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 34 KB 👁 1 views

Synthesis of Protected Hexp-(1 → 4)-β-D-GlcpNAc-(1 → 2)-α-D-Manp-(1 → O)(CH2)7CH3 Sequences (Hex: β-D-Glc, 4-deoxy-4fluoro-β-D-Gal, or 4-deoxy-β-D-Gal) Using a Glc-GlcNPhth Donor, Eventually Fluorinated or Deoxygenated at the Oligosaccharide Level. -The title trisaccharide derivatives are prepared