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A new practical synthesis of silyl enol ethers : Part.I. From simple aldehydes and ketones

โœ Scribed by P. Cazeau; F. Duboudin; F. Moulines; O. Babot; J. Dunogues

Publisher
Elsevier Science
Year
1987
Tongue
French
Weight
824 KB
Volume
43
Category
Article
ISSN
0040-4020

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โœฆ Synopsis

OO4o-l020/87 s3.00+ .@I Q 1987 Pergamon Joumsls Ltd.

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Various chlorodifluoromethyl ketones can be converted to the corresponding 2,2-difluoro enol silyl ethers in good yields, by the action of zinc dust and chlorotrimethylsilane in dry acetonitrile at 60ยฐC. Since the findings of improved methods for the preparation of enol silyl ethers, 1 it has well b

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Enol boranes, I, undergo efficient exchange with N-trimethylsilylimidazole, 2, to afford the corresponding trimethylsilyl enol ethers, 3, in good yield under mild conditions. Synthetic routes to enol silyl ethers and enol boranes have received considerable attention recently because of their importa