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A new organic-inorganic molybdenum arsenate complex based on [(CuO6)(As3O3)2Mo6O18]4- cluster as secondary building units

✍ Scribed by Fangyong Su; Baibin Zhou; Zhifeng Zhao; Zhanhua Su; Chuncheng Zhu

Publisher: John Wiley and Sons
Year: 2009
Tongue: English
Weight: 233 KB
Volume: 44
Category: Article
ISSN: 0232-1300
DOI: 10.1002/crat.200800542

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✦ Synopsis

, has been synthesized under mild hydrothermal conditions, and characterized by elemental analysis, IR, thermogravimetric analyses, and single-crystal X-ray diffraction analysis. The polyanion framework derives from the Anderson structure in which the central octahedron is filled up by a copper (II), and is capped on both sides by two cyclic As 3 O 6 groups. The countercations contain bisupported [Cu(imi) 2 ] + complex cations and two free [Cu(imi) 2 ] + complex cations. The electrochemical behavior of 1-modified carbon paste electrode (1-CPE) has been studied in detail.

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