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A New Method for the Synthesis of Nonsymmetrical Sulfamides Using Burgess-Type Reagents.

✍ Scribed by K. C. Nicolaou; Deborah A. Longbottom; Scott A. Snyder; Annie Z. Nalbanadian; Xianhai Huang

Publisher
John Wiley and Sons
Year
2003
Weight
151 KB
Volume
34
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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## Abstract The 1‐(3‐methylazulen‐1‐yl)alkan‐1‐ones, when oxidized with excess 2,3‐dichloro‐5,6‐dicyano‐1,4‐benzoquinone (=4,5‐dichloro‐3,6‐dioxocyclohexa‐1,4‐diene‐1,2‐dicarbonitrile; DDQ) in aqueous acetone in the presence of 1‐(3‐demethylazulen‐1‐yl)alkan‐1‐ones, form the corresponding unsymmetr