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A new facile oxidation of sulfides to sulfoxides

✍ Scribed by Masaru Hojo; Ryōichi Masuda

Book ID
108380078
Publisher
Elsevier Science
Year
1976
Tongue
French
Weight
129 KB
Volume
17
Category
Article
ISSN
0040-4039

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📜 SIMILAR VOLUMES

Highly Enantioselective Oxidation of Sul
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An efficient asymmetric oxidation of sul
An efficient asymmetric oxidation of sulfides to sulfoxides
✍ Philippe Pitchen; Henri B. Kagan 📂 Article 📅 1984 🏛 Elsevier Science 🌐 French ⚖ 240 KB

The Sharpless reagent (Ti(OiPr)4 t 1 mol eq. diethyl tartrate (DET) t 2 J-BuOOH) modified by addition of one mol eq. H20 gives a new homogeneous reagent which cleanly oxidizes sulfidesinto sulfoxides in dichloromethane. The best results were obtained for the stoichiometry Ti/DET/ H20/J-BuOOH = 1:2:1