A new efficient route to 3-vinylthiophene
✍ Scribed by Maël Nicolas; Bruno Fabre; Jean-François Pilard; Jacques Simonet
- Publisher
- Journal of Heterocyclic Chemistry
- Year
- 1999
- Tongue
- English
- Weight
- 92 KB
- Volume
- 36
- Category
- Article
- ISSN
- 0022-152X
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✦ Synopsis
Abstract
The synthesis of 3‐vinylthiophene was efficiently achieved in two steps. 3‐(2‐bromoethyl)thiophene prepared from 3‐(2‐ethanol)thiophene was converted to the title compound (70% overall yield) using tetraglyme as a solvent and 1,8‐diazabicyclo[5.4.0]undec‐7‐ene as a base.
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