Iodometric Estimation of Acetylacetone i
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LΓ‘szlΓ³ J. CsΓ‘nyi; KΓ‘roly JΓ‘ky
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Article
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1997
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Elsevier Science
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English
β 94 KB
The iodoform reaction is recommanded for the estimation of acetylacetone. In 20 ml moderately alkaline buffer solution, 0.04-0.40 mmole acetylacetone is oxidized with 15-20 ml 0.2 N KI 3 solution at a sufficiently slow delivery rate (0.03 mlrs 01 or less) under efficient stirring during addition of