A new convenient method of azide condensation
β Scribed by L. Y. Alfeeva; L. A. Andreeva; V. N. Nezavibat'ko
- Publisher
- Springer Netherlands
- Year
- 1995
- Tongue
- English
- Weight
- 138 KB
- Volume
- 2
- Category
- Article
- ISSN
- 1573-3149
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β¦ Synopsis
A new convenient modification of azide condensation is evaluated. The modification includes the use of tetrabutylammonium nitrite and p-toluene sulphonic acid, which are easily dissolvable in organic solvents, for the acidification of the reaction mixture.
π SIMILAR VOLUMES
A new facile method for monoacylation of diols has been developed. A variety of cyclic and acyclic diols, in particular 1,2-diols, was selectively monobenzoylated in good yields by their reaction with benzoyl chloride in the presence of a catalytic amount of dimethyltin dichloride and inorganic base
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